Digitalization-it, Industry-4-0-it 4 Marzo 2022

Mitigate variations and optimise critical product parameters?

hiperespectral NIR spectroscopy donuts fat content nir
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In this article we will address two recurring issues in food production: mitigating variations in the physical-chemical composition of the product by controlling critical nutritional values and how these parameters can be optimised with online tools. Finally, we will address a case of application of hyperspectral NIR technology within the industrial bakery sector and the control of a critical input in this industry, fat.

nir hiperespectral

The Hyperspectral technology discussed in this article is an extension of traditional artificial vision in two ways: Firstly, instead of the usual three colour channels in artificial vision, hyperspectral imaging uses up to hundreds of channels, making it possible to see very subtle differences. Secondly, hyperspectral cameras often have an extended spectral range beyond the visible, i.e. into the infrared, where the chemical composition is much more evident than in the visible range. Therefore, hyperspectral imaging can be seen as a paradigm shift in vision systems and as a source of abundant, high-quality data to feed vision systems based on artificial intelligence algorithms. In practice, having a hyperspectral camera is equivalent to having a spectrophotometer in every pixel.

Until now, however, the use of this technology has been limited to very specific environments: military applications and research laboratories. IRIS is a pioneer in extending the use of this technology beyond such environments, in order to exploit its enormous potential in industrial environments. In this sense, it is not enough to have a suitable camera, but each specific application requires integration work and the development of the appropriate machine learning solution. IRIS specialises in both areas.

While the technology has numerous applications in different industries and processes, we will talk about the industrial bakery sector, where it is essential to control the fat content, not only because consumption trends demand it, but also because large variations in the fat value result in cost overruns, explained by the suboptimal use of the raw material – oil – as well as unexpected changes in the palatability of the product when the input is well above or below the optimal value.

What happens is that, with current laboratory techniques to control the fat value, such as the Soxhlet method, which involves several hours, it is never possible to notice these variations and rectify the process in real time, as it is an off-line method, which requires specific sampling, preparation, inputs and personnel and especially time for its results, This makes it incompatible with the idea of standardising the product, the use of raw materials and particularly with any attempt to optimise the critical quality parameters in the production process, which can only be done by having continuous measurement – and information – and a minimum margin of error.

The latter is interesting to clarify and happens with different parameters in different foods that are manufactured, such as moisture, fat, sugars, seasonings or others, where there is an “optimal” value in the quality vs. production costs equation, but difficult to achieve due to the lack of real time measurement and information of the chemical composition of the product. For example, if as a manufacturer, I know the moisture value of my production in real time and the error of that measurement is very low, there is margin and possibility to adjust the formulation of the product to that ideal value; otherwise, with an off-line method, it would be a high risk decision and difficult to control.

An application case:

A major customer in the industrial bakery sector needed to mitigate variations in fat content and optimise its use in the process. Changes in the product were observed that could hardly be explained by formulation changes. Therefore, a study was started to see which processes were producing these changes. The study is slow and complicated because he lacks a tool that allows him to quickly measure the fat content in order to be able to relate it to changes in his processes.

 

The installed industrial Visum HSI™ system operates in the infrared range. It allows inspection in terms of fat content on a unit-by-unit product basis. IRIS Technology Solutions’ integrated software and chemometrics tools enable the user to self-calibrate the device to changes in product composition and it is seamlessly interfaced with plant information systems.

As a result, the client was able to determine the point in the process where fat variations were generated by measuring and adjusting in real time the recipe and save 1.5% of oil in the process.

Like all IRIS Technology equipment, it is multi-parametric, so it can simultaneously provide, based on the same reading, information on multiple parameters, not only quantitative (e.g. moisture or sugar content or unit size), but also qualitative (e.g. degree of cooking or morphological variations).

 

If you want to know more about NIR spectroscopy hiperespectral and its applications to other processes, products and industries, please contact us at info@iris-eng.com.

Di IRIS Technology Solutions
Industry-4-0-it, Innovation-it 24 Gennaio 2022

IRIS Technology develops the first industrial system for the chemical control and inspection of melamine boards

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IRIS Technology, a Spanish engineering company that manufactures photonic solutions for online quality control, has developed the first industrial system for real-time quality control of melamine or particle boards with NIR and hyperspectral technology.

 

The wood industry, and consequently the furniture and furnishing industry, is a sector that continues to grow by leaps and bounds worldwide, with a year-on-year increase of 6.5%, still boosted by the increase in consumption during the pandemic. So, not surprisingly, technology is accompanying the industry in this growth by combining production and operations techniques with smart technologies such as photonics, analytics and artificial intelligence brought about by Industry 4.0.

 

The new chemical vision industrial system, manufactured and patented by IRIS Technology, uses NIRS (Near Infrared Spectroscopy) technology and machine learning together with chemometric models to analyse the composition of each melamine board unit produced, non-invasively, It can quantitatively analyse the distribution of the moisture parameter on the impregnation line and classify the curing level of each board in order to detect defects early, correct factory processes and reject or remanufacture boards.

 

Until now, the control of this type of parameters in the melamine production process was only carried out through destructive laboratory methods and visual inspection, implying a high cost for the manufacturer and the difficult -if not impossible- inspection of all the units produced. This new technological application stands as a solution for the inspection of this type of boards, thus reducing defective units, losses, claims and consequently improving the brand image of the manufacturer.

 

For more information please contact IRIS Technology www.iris-eng.com

Contrôle des produits chimiques
Di IRIS Technology Solutions
Digitalization-it, Industry-4-0-it 20 Gennaio 2022

Real-time Brix control with NIR technology: a competitive factor for production and commercialisation.

Contrôle du degré Brix
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In the fruit and vegetable industry, as well as for fruit products (juices, purees, concentrates, among others), a critical value either to determine quality standards, commercialisation, ripeness or to adjust the recipe of certain food preparations, are the Brix degrees. In this article we will talk about this, how this control is currently carried out in certain industries and how Brix degrees can be controlled in real time with NIR technology and its benefits.

 

The Brix degree (ºBx) is a parameter strongly correlated with the content of soluble solids and, in particular, sugars, therefore, and because it is relatively easy to measure, it is often used as a process and quality control criterion. In many cases, the acceptance criterion for semi-products and products is simply based on a certain threshold value expressed in Brix.  In the case of fruits, the quotient of Brix to total acidity is the usual, and even legal, criterion for determining the degree of ripeness.

 

Currently, in the vast majority of the industry, this ºBx control is carried out by traditional laboratory methods, where “representative” samples are taken from a batch and subjected to a conventional destructive technique such as refractometry or HPLC analysis. This traditional method, in addition to having a cost (of specialised personnel, time and equipment), is not sufficient to cope with the high variability in the quality attributes present in fruit and vegetable batches, nor with the need of the fruit and vegetable processing industry to monitor this parameter in real time and be able to adjust the other components of the “recipe” of its product, according to the parameter of interest. In other words, monitoring this parameter online for the processing industry means optimising all process inputs and standardising the quality of the final product. For fruit and vegetable growers, analysing ºBx with a portable Visum Palm™ NIR analyser, for example, is useful to save laboratory time, determine their marketability and even improve the terms of trade with their customers and guarantee more quality to the domestic and export market. At the same time, a NIR analyser, in any of its versions, is capable of performing, depending on its concentration, added measurements such as total acidity, pH and the concentration of other analytes of nutritional or organoleptic interest.

 

An application case

A major producer of fruit-based food preparations, occasionally enriched with dairy products, in order to be able to standardise its products to meet the requirements of its customers – supermarket chains – requested an in-line solution, flexible enough to be compatible with its wide range of products.

 

This solution, based on a Visum NIR In-Line™ analyser for liquids, included not only the Visum In-Line hardware and its adaptation to the characteristics of its line, but also at software level the development of a library of predictive models capable of continuously determining the Brix and pH of different “families” of products with respective maximum inaccuracies of 0. 5 for ºBx and 0.1 pH, which constituted a global and adequate solution for making technological decisions in real time to guarantee the standardisation of the product and its quality within the limits required by the client.

Di IRIS Technology Solutions

In the industrial bakery and pastry sector, the moisture of bread and pasta doughs is a parameter that requires exhaustive control, since changes in product moisture affect phenomena such as honeycombing, type of crust, or consistency, as well as alterations in conservation and the effect of time during the supply chain, from the factory to the end consumer. In this article we will talk about real-time moisture monitoring, the scope of infrared spectroscopy (NIR) at different points of the process and we will share an application case of automatic control in the manufacture of toast at the exit of the oven.

The current reference laboratory method for determining the % moisture content is the gravimetric method, which consists of drying a sample and measuring the weight loss (water difference). This method can take from several minutes to hours if stoves are used. It is therefore a resource-intensive method (personnel, equipment, materials and time) that directly affects efforts and the possibility of being able to optimize the nutritional parameter – moisture – of the product.

In the bread and bakery industry, moisture references are obtained at different stages of the manufacturing process in order to ensure compliance with standardized quality criteria, which can be synthetically grouped as follows:

Quality control of raw materials and ingredients. They can be used to verify that raw material arrivals are in compliance and to verify the quality of whole and milled grains, which affects the quality of the final product.

Quality control of bakery mixes and doughs. They can be used during production to measure flour yield, water absorption during the milling process, dough fermentation time and to determine the composition of the baking mix (% moisture, protein and ash).

Quality control of finished products. They can be used to control the quality of the finished product at the end of production or on the packaging line, ensuring compliance with legal compositional requirements, or provide data for nutritional labeling.

NIR (near infrared) technology is able to optimize all measurements in real time, either by monitoring with a portable analyzer, as in the case of the Visum Palm™, or by ensuring continuous control on the conveyor belt, cooler, or in the mixing tank with a Visum NIR In-Line™ analyzer, working in this case connected to the line’s management systems and PLC to control the manufacturing process or rectify in real time any malfunctions.

An application case, control of the baking process.

A mini-toast manufacturer needed a method to determine the humidity of the toast at the oven exit in real time, to mitigate the effects of the analysis time variable that made it impossible to rectify the baking temperature and therefore lost production batches that were not in accordance with the manufacturer’s specifications.

The problem of humidity in toast is that when humidity values are below 3.5%, the toast is fragile and tends to break during transport or handling, and when humidity is above 4.5%, the toast loses its crispiness. Continuous NIR technology makes it possible to optimize the parameter of interest.

For practical purposes, a predictive moisture model was made from samples and reference values from the customer’s laboratory, and since infrared spectroscopy is particularly sensitive to the presence of water, the same model could at the same time predict moisture in different varieties of the same customer’s product. The resulting model has a correlation coefficient close to 1 (0.99), indicating its accuracy. Connected to the PLC, the system identifies the product and instantly configures the analyzer to monitor the parameter of interest.

Finally, a Visum NIR In-Line™ continuous NIR analyzer was installed on the conveyor belt at the oven exit to determine the moisture value per area and, connected to the oven PLC, to rectify the burner temperature and provide real-time process/product information.

Instead of working with Vis-NIR, with the Visum HSI™ NIR (900-1700 nm) it would have been possible to analyze product unit by product unit, adding to the moisture analysis parameters such as color, homogeneity of components, spatial distribution of components, detection of foreign bodies (metals, plastics, cartons, etc.) or other critical process parameters. Needless to say that a single analyzer can perform countless predictions simultaneously, moisture, fats, proteins, sugars, etc. But this was not the case, we will tell you about it in another article.

I hope you have found this article on moisture monitoring with on-line NIR spectroscopy useful and we invite you to send us your comments and suggestions to our e-mail address news@iris-eng.com.


Joel Valdés Bravo
Technical Disclosure
IRIS Technology | Visum

 

Di IRIS Technology Solutions
Industry-4-0-it, Innovation-it, Pharma-4-0-it 27 Ottobre 2021

Pre-release: The new Visum Raman analyzer will go on pre-sale to a small number of pharmaceutical companies.

Le nouvel analyseur raman
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IRIS Technology presents in the latest edition of Farmespaña Industrial Magazine – Farmaforum Special – its line of PAT analyzers for the pharmaceutical industry with a great novelty for the industry, the expectation for the launch of its Raman analyzer, which will be available both to work at-line or integrated to the line, for the beginning of next year, and whose official launch will begin with a pre-sale stage to a limited number of Spanish pharmaceutical companies.

 

“Our industry knowledge and PAT experience have led us to develop this new member of our Visum family of spectroscopic analyzers, mainly to meet many needs for in-line formulation control, where the particularities of each project and the chemometric modeling work behind each one of them is extremely complex,” said Alejandro Rosales, Science and Technology Manager at IRIS.

 

IRIS Technology’s technical teams are currently working on expanding Raman analyzer applications to processes at different stages of the drug manufacturing industry prior to launch, and invite pharma companies interested in particular applications to perform ad-hoc modeling at no cost.

 

Visum Raman achieves a signal-to-noise ratio far superior to its market competitors because, thanks to its temporal resolution, it physically mitigates the undesirable effects of fluorescence, making it possible to extend the range of applications in the pharmaceutical industry beyond identification.

 

“It is important to us that the Visum Raman, like its NIR siblings, is strongly oriented to the process and production industry, and helps operators and technicians in the factory to make technological decisions at the line and in real time. For this reason, we have already been collaborating with some companies in response to particular challenges, but with a strong transversality to other products and processes. In relation to the reasonable technological uncertainty that this type of industrial-scale projects always generate, at IRIS we work under the “proof of concept” scheme, i.e., we previously validate the success of the project on a reduced scale and in comparison with the criteria agreed with the client”, remarked the Deputy Director of IRIS, Joan Puig.

 

Do you have a challenge for our Raman analyzers? Do you want to participate in the pre-sale? Write to us here.

 

Di IRIS Technology Solutions

IRIS Technology presents in Farmespaña Industrial applications of its PAT analyzers for the pharmaceutical and dermo-cosmetic industry.

Real-time content uniformity.

Real-time bioavailability.

Fluorescence-free Raman.

Read the complete note here.

Di IRIS Technology Solutions
Digitalization-it, Industry-4-0-it 9 Settembre 2021

IRIS presents at Expoquimia 2021 its NIR and Raman applications for on-line process control.

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Next Wednesday September 15 at 10 am, in the framework of the panel organized by ACCIÓ at Expoquimia called “Industry 4.0 Marketplace in the chemical, plastics and pharmaceutical sectors”, Joan Puig, Deputy Director of IRIS, will present some relevant industrial projects where NIR and Raman spectroscopy has been applied in integrated solutions to production lines in real time.

Both spectroscopic techniques (NIR and Raman) that IRIS works with and incorporated in its Visum® line of devices promote the digitization of quality and process control, without the need to resort to traditional laboratory and sampling techniques, and have a direct impact on time-to-market and quality standardization throughout the entire production process.

Di IRIS Technology Solutions
Digitalization-it, Industry-4-0-it 22 Giugno 2021

VISUM® at the first edition of Food 4 Future FoodTech Bilbao 2021

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Last week, the VISUM® team participated in Food 4 Future in Bilbao, where the entire food and beverage industry was invited. In parallel, networking activities and the Congress took place, where Alejandro Rosales, Science and Technology Manager at IRIS presented “Spectroscopy and machine learning: 4.0 tools for process control and food safety”.

It is important to highlight the growing interest of the industry in the digitization of processes, including those aimed at optimizing quality and making costs more efficient.

 

Di IRIS Technology Solutions
Digitalization-it, Industry-4-0-it 26 Maggio 2021

IRIS will participate in FoodTech: FOOD 4 FUTURE – BILBAO 2021 | June 15 – 17

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After a long break of physical social interaction and with recharged energies, we are back to the big trade shows and conventions of the year, this time, participating in FoodTech: Food 4 Future (F4F), which will take place at the Bilbao Exhibition Center, in Bilbao, from June 15 to 17.

F4F condenses the offer of technological innovation and industry 4.0 for the food chain and is the meeting place of this 2021 for all professionals or technicians in the sector. Whether to learn about the most innovative solutions to promote the digital transformation of the company, to return to networking -real-, or to participate in the Food 4 Future World Summit, the largest European congress on innovation technology in the food and beverage industry.

 

Where to find us?

We will be present at Stand F620 in Hall 1 of the exhibition center. You will also be able to listen to us as speakers at the Congress, where our Science and Technology Manager, Phd. Alejandro Rosales, will talk about “Spectroscopy and machine learning 4.0 tools for process control and food safety”.

 

We are waiting for you!

Di IRIS Technology Solutions
Industry-4-0-it, Innovation-it 14 Maggio 2021

IRIS Technology among the Top 10 Spanish mechanical engineering startups of 2021

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The company IRIS Technology, is awarded in the ranking “Top Mechanical Engineering Startups in Spain 2021”, elaborated by the British portal “startupill.com“, in the position Nº6 of the most innovative companies in the mechanical engineering industry and worth following this year.

Startupill.com bases its selection on the performance of companies in categories such as: innovation, innovative ideas, innovative route to market, innovative product, growth, exponential growth, exponential growth strategy, management and social impact. Look the entire publication here.

About IRIS Technology

IRIS (www.iris-eng.com) is an advanced engineering company that manufactures PAT systems for in-line process and quality control in the pharmaceutical, food and chemical industries with its own devices registered under the VISUM Devices trademark. As a manufacturer, it realizes tailor-made solutions and ad-hoc configurations for different processes and analytical or control needs, from the actual engineering development to the specific chemometric modeling. In addition, it actively collaborates in numerous EU innovation projects with international partners and has in its staff physicists, mathematicians, chemometricians, opticians, engineers, software developers and highly specialized profiles from the world of science and technology.

Di IRIS Technology Solutions